Efforts to produce BAR lipid by conventional means were met with frustration, low conversion was observed due to residual H2O promoting by product formation. BAR lipid was resolved chromatographically, but low conversion led to alternative strategies being explored which ultimately proved unsuccessful. An alternative strategy involving a one pot Knoevenagel condensation proved promising on a test substrate, but the aldehyde precursor required for BAR lipid formation was not producible.
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